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- MakaleYalnız künye2025Scopus SJRQ1Sensitive Microwave Sensor for Detection and Quantification of Water in Adulterated Honey
Hasar, Hafize; Hasar, Ugur Cem; Kaya, Yunus; Ozturk, Hamdullah; Korkmaz, Huseyin; Yuzgulec, Kadir; Karaaslan, Muharrem; Ebrahimi, Amir; Nayyeri, Vahid; Ramahi, Omar M.
Honey is a rich source of sugar and is one of the indispensable ingredients in infant foods. Thus, it can be subjected to adulteration due to its cost. Measurement techniques such as liquid chromatography and near-infrared spectroscopy, used for detecting any adulteration, are expensive and need to be conducted by highly trained personnel for off-line analysis. Microwave measurements, as a fast, simple, and relatively inexpensive analysis, have recently shown great potential in detecting adulteration within honey samples. Nonetheless, sensor types used in such measurements are conventional. In this study, a reflection-type sensitive microwave sensor terminated by a metal back is proposed for the first time in the literature for the detection and quantification of water percentage ( delta ) level (mass-to-mass basis) within water-adulterated honey samples. When compared with other resonance-based microwave cavity sensors, thanks to its eight strips located at the centers of two closed circular loops, it demonstrates superior frequency selectivity and sensitivity ( S=5.13 %) validated by full-wave 3-D simulations performed by the CST Microwave Studio and equivalent circuit analysis carried out by the Advanced Design System (ADS) software. For example, for ethanol, the proposed sensor gives a frequency shift of more than 1 GHz in the X band. Resonance frequency shift and variation of the reflection coefficient amplitude ( |S11| ) are measured at X band to detect honey samples with up to 8% adulteration level. Three different honey samples (flower honey, highland honey, and thyme honey) were examined to test the performance and applicability of the proposed sensor.
AtıfScopus18WoS14OpenAlex17
İncele - MakaleAçık Erişim2024Scopus SJRQ1Simple and inexpensive microwave setup for industrial based applications: Quantification of flower honey adulteration as a case study
Hasar, Ugur C.; Hasar, Hafize; Ozturk, Hamdullah; Korkmaz, Huseyin; Kaya, Yunus; Ozkaya, Mehmet Akif; Ebrahimi, Amir; Barroso, Joaquim J.; Nayyeri, Vahid; Ramahi, Omar M.
A simple and inexpensive microwave measurement setup based on measurements of magnitudes of transmission properties ( | S 21 | dB \documentclass[12pt]{minimal} \usepackage{amsmath} \usepackage{wasysym} \usepackage{amsfonts} \usepackage{amssymb} \usepackage{amsbsy} \usepackage{mathrsfs} \usepackage{upgreek} \setlength{\oddsidemargin}{-69pt} \begin{document}|S₂₁|_dB\end{document} ) is proposed for industrial-based microwave aquametry (moisture or water content) applications. An easy-to-apply calibration procedure based on normalization is implemented to eliminate systematic errors in the measurement system. As a case study, we applied this setup for the quantification of water-adulteration in flower honey. After validating this system by distilled water and pure flower honey measurements, | S 21 | dB \documentclass[12pt]{minimal} \usepackage{amsmath} \usepackage{wasysym} \usepackage{amsfonts} \usepackage{amssymb} \usepackage{amsbsy} \usepackage{mathrsfs} \usepackage{upgreek} \setlength{\oddsidemargin}{-69pt} \begin{document}|S₂₁|_dB\end{document} measurements of the pure flower honey with various adulteration percentages ( delta \documentclass[12pt]{minimal} \usepackage{amsmath} \usepackage{wasysym} \usepackage{amsfonts} \usepackage{amssymb} \usepackage{amsbsy} \usepackage{mathrsfs} \usepackage{upgreek} \setlength{\oddsidemargin}{-69pt} \begin{document}δ\end{document} ) up to 9% are conducted to examine the performance of the measurement setup for quantification of water adulteration. A multi-dimensional fitting procedure is implemented to predict delta \documentclass[12pt]{minimal} \usepackage{amsmath} \usepackage{wasysym} \usepackage{amsfonts} \usepackage{amssymb} \usepackage{amsbsy} \usepackage{mathrsfs} \usepackage{upgreek} \setlength{\oddsidemargin}{-69pt} \begin{document}δ\end{document} using the proposed inexpensive microwave measurement setup. It is shown that it is possible to quantify an adulteration level with an accuracy better than -/+ 1 \documentclass[12pt]{minimal} \usepackage{amsmath} \usepackage{wasysym} \usepackage{amsfonts} \usepackage{amssymb} \usepackage{amsbsy} \usepackage{mathrsfs} \usepackage{upgreek} \setlength{\oddsidemargin}{-69pt} \begin{document}∓ 1\end{document} % by the proposed measurement setup and the applied multi-dimensional fitting procedure.
AtıfScopus12WoS10OpenAlex15
İncele - MakaleYalnız künye2023Scopus SJRQ1Honey-Water Content Analysis by Mixing Models Using a Self-Calibrating Microwave Method
Hasar, Hafize; Hasar, Ugur C.; Kaya, Yunus; Ozturk, Hamdullah; Izginli, Mucahit; Oztas, Taskin; Aslan, Nevzat; Ertugrul, Mehmet; Barroso, Joaquim J.; Ramahi, Omar M.
Microwave techniques, as an indirect approach, can be applied for analyzing water content in honey by way of permittivity measurements. However, these techniques require proper calibration to accurately perform such indirect evaluation. Improper calibration standards used in this calibration process could naturally result in a reduction in the accuracy and thus the performance of dielectric characterization using microwaves. Self-calibrating microwave techniques can reduce the effects of imprecise standards and thus improve the performance of microwave measurements by bypassing the requirement of calibration standards. In this study, we develop a self-calibrating microwave measurement technique to determine the relative permittivity of honey samples and implement binary mixing models to predict adulteration levels of water-adulterated honey. From this implementation, it is observed that the parallel-capacitance mixing model could efficiently be applied to determine the concentration of water adulteration by examining the differences between absolute values of the real parts of the measured and predicted complex permittivities of adulterated honey.
AtıfScopus18WoS16OpenAlex18İncele - MakaleYalnız künye2023Scopus SJRQ1Temporal Reflection Response of Plane Waves Within an N-Layer Structure Involving Bianisotropy
Hasar, Ugur C.; Ozturk, Gokhan; Kaya, Yunus; Barroso, Joaquim Jose; Ertugrul, Mehmet; Ramahi, Omar M.; Alfaqawi, Mona S. S.
The temporal reflection response of an N-layer composite structure involving bianisotropic behavior is examined for the first time in the literature. Toward this goal, the wave matrix (WM) method, which is fundamental, relatively easier to apply, and compact and iterative suitable for analysis of multilayer structures, is first extended to the analysis of an interface separating two different media involving bianisotropy. Next, the reflection response of the whole structure is derived in terms of series form to better analyze its temporal behavior. Then, frequency-domain and time-domain responses of the whole structure are expressed using a special reflection coefficient (the reduced reflection coefficient) by way of the concept of subregions. A numerical analysis is performed to demonstrate the applicability of our formalism for two different polarization types (perpendicular and parallel).
AtıfScopus3WoS3OpenAlex3İncele - MakaleYalnız künye2023Scopus SJRQ1Extraction Method for Unique Determination of Complex Permittivity From Graphical Analysis of Natural Frequencies
Hasar, Ugur C.; Ozturk, Gokhan; Kaya, Yunus; Alfaqawi, Mona S. S.; Barroso, Joaquim Jose; Ertugrul, Mehmet; Ramahi, Omar M.
A time-domain free-space extraction procedure is proposed to uniquely determine the relative complex permittivity epsilon(r)(omega) based on two sets of natural frequencies of the metal- and air-backed dielectric samples. A graphical analysis is applied for evaluating whether unique epsilon(r)(omega) can be extracted using such natural frequencies. The method is numerically validated using two dielectric samples with different epsilon(omega) for the ideal case (no noise) and under the influence of noise with different signal-to-noise ratios (SNRs).
AtıfScopus1OpenAlex1İncele - MakaleAçık Erişim2022Scopus SJRQ1Broadband Soil Permittivity Measurements Using a Novel De-Embedding Line-Line Method
Hasar, Hafize; Hasar, Ugur C.; Kaya, Yunus; Oztas, Taskin; Canbolat, Mustafa Y.; Aslan, Nevzat; Ertugrul, Mehmet; Ramahi, Omar M.
A new de-embedding line-line method has been proposed for accurate complex relative permittivity ( ε ᵣ ) determination of soil samples loaded into an EIA 1-5/8' coaxial transmission line measurement system. The method has three main features. First, it bypasses the requirement of calibration of this system by using only two identical coaxial lines with different lengths. Second, it does not need any numerical technique for ε ᵣ determination. Third, it does not require knowledge of electromagnetic properties and thickness information of the bead used for supporting soil samples. The method is next validated by simulations performed using a full 3-D electromagnetic simulation program (CST Microwave Studio) and by ε ᵣ measurement of a polyethylene (PE) material. Finally, ε ᵣ values of three air-dried and water-saturated soil samples having 90% or more sand content with different electrical conductivities (ECs) and gathered from different areas of the city Gaziantep in Turkey, were measured.
AtıfScopus18WoS16OpenAlex16İncele - MakaleAçık Erişim2022Scopus SJRQ1Improved Method for Permittivity Determination of Dielectric Samples by Free-Space Measurements
Hasar, Ugur Cem; Kaya, Yunus; Ozturk, Hamdullah; Izginli, Mucahit; Ertugrul, Mehmet; Barroso, Joaquim Jose; Ramahi, Omar M.
A new deembedding technique is proposed for relative complex permittivity epsilon(r) determination of dielectric materials using gated free-space measurements. Its three main features are 1) it does not require any formal calibration procedure (calibration-free); 2) it is position-insensitive; and 3) it extracts ripple-free epsilon(r) due to gating process. The objective function derived to determine epsilon(r) by the proposed method is validated by free-space measurements of three dielectric samples (polypropylene, polyethylene, and polyoxymethylene). Besides, the accuracy of our method is compared with the accuracy of other calibrationfree and calibration-dependent methods in the literature.
AtıfScopus49WoS36OpenAlex44İncele - MakaleAçık Erişim2022Scopus SJRQ1Determination of Propagation Constants and Wave Impedance of Non-Reciprocal Networks From Position-Insensitive Waveguide Measurements
Hasar, Ugur C.; Kaya, Yunus; Izginli, Mucahit; Ozturk, Hamdullah; Barroso, Joaquim J.; Ramahi, Omar M.; Ertugrul, Mehmet
A microwave method is proposed to determine the forward and backward propagation constants (gamma ⁺ and gamma ⁻) and the wave impedance ( z_w ) of reciprocal and non-reciprocal microwave networks whose positions are not known within their measurement cells (position-insensitive). The proposed method relies purely on analytical expressions and can also evaluate the reference plane transformation distances. Scattering parameter measurements at the X-band (8.2-12.4 GHz) of a reciprocal network (a waveguide straight) and a non-reciprocal network (a microwave phase shifter) arbitrarily positioned into their measurement cells were conducted to retrieve gamma ⁺, gamma ⁻, and z_w for validation of our method and testing its position-insensitive property. The importance of the method becomes apparent when compared to conventional methods whose accuracy is based on precise determination of the reference planes.
AtıfScopus9WoS9OpenAlex9İncele - MakaleYalnız künye2022Scopus SJRQ1Complex Permittivity and Thickness Evaluation of Low-Loss Dielectrics From Uncalibrated Free-Space Time-Domain Measurements
Hasar, Ugur Cem; Kaya, Yunus; Ozturk, Hamdullah; Izginli, Mucahit; Barroso, Joaquim Jose; Ramahi, Omar M.; Ertugrul, Mehmet
A free-space time-domain method is proposed to retrieve dielectric constant (epsilon r), conductivity (sigma e), and thickness (d) of metal-backed low-loss dielectric samples using calibration-independent reflected power peak measurements. Its algorithm is validated by numerical calculations and simulations (CST Microwave Studio) using a sine-modulated Gaussian window. A sensitivity analysis is followed to examine its performance considering the dependencies of reflected power peaks with respect to epsilon r and sigma e. Free-space time-domain measurements have been implemented after transforming frequency-domain measurements into time-domain ones to extract epsilon r, sigma e, and d of polypropylene, polyethylene, and polyoxymethylene samples.
AtıfScopus48WoS42OpenAlex43İncele - MakaleYalnız künye2022Scopus SJRQ1Feasible Extraction Method for Electromagnetic Properties of Multilayer Metamaterials With Short-Circuit Termination
Hasar, Ugur Cem; Ozturk, Gokhan; Kaya, Yunus; Bute, Musa; Karaaslan, Muharrem; Barroso, Joaquim J.; Ramahi, Omar M.; Ertugrul, Mehmet
An extraction technique is proposed for electromagnetic characterization of metal-backed multilayer metamaterial (MM) structures demonstrating reflection-asymmetric property. It uses recursive scattering parameters for direct and reversed configurations of a multilayer structure. The algorithm was validated by comparing the extracted electromagnetic properties of multilayer structures composed of different MM unit cells with those determined by one-layer-only S-parameter methods. Two-layer and three-layer multilayer structures composed of MM slabs with C-shaped and Omega-shaped rings and an FR4 material were fabricated and measured for experimental validation. A sensitivity analysis was also conducted to quantitatively evaluate the performance of our method against a small air gap between the multilayer structures and the short-circuit termination and between adjacent MM slabs within these structures. Strong agreement was observed between the resulted obtained using our method and measurements.
AtıfScopus10WoS10OpenAlex10İncele - MakaleAçık Erişim2021Scopus SJRQ1Coupling analysis between resonating metamaterial slabs using scattering parameters
Hasar, Ugur Cem; Kaya, Yunus; Izginli, Mucahit; Ozturk, Hamdullah; Ertugrul, Mehmet; Ramahi, Omar M.
Metamaterial (MM) slabs in close proximity can couple with one another. This coupling can modify the electromagnetic response of the overall MM structure involving individual MM resonators. The signal flow graph technique along with the ABCD parameters are applied to quantitatively and qualitatively examine this coupling from simulated/measured scattering parameters of cascade connection of closely or largely separated MM slabs. S-parameter measurements of a MM slab constructed by split-ring-resonators were carried out at X-band (8.2-12.4 GHz) to validate our theoretical analysis.
AtıfScopus2WoS2OpenAlex2İncele