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- MakaleYalnız künye2026Scopus SJRQ4SURFACE ROUGHNESS AND SHORE-D HARDNESS OF SIX TROPICAL HARDWOODS; [RUGOSIDADE DA SUPERFÍCIE E DUREZA SHORE-D DE SEIS MADEIRAS TROPICAIS]; [RUGOSIDAD SUPERFICIAL Y DUREZA SHORE-D DE SEIS MADERAS TROPICALES]
Ayata, Umit; Domingos, Idalina; Ferreira, José; Cruz-Lopes, Luísa; Esteves, Bruno
Introduction: This study investigates the Shore-D hardness and surface roughness characteristics of six tropical wood species: Canelo (Nectandra spp.), Limbali (Gibertiodendron dewevrei), Difou (Morus mesozygia), Curupay (Anadenanthera macrocarpa), Ebiara (Berlinia bracteosa), and Zwarte kabbes (Diplotropis martiusii), aiming to assess their suitability for high-performance applications. Objective: To evaluate how wood species and sanding processes influence the mechanical properties and surface quality of selected tropical woods. Methods: Samples were conditioned and sanded using abrasives of different grit sizes (80, 100, 120, 150, and 180). Surface roughness parameters Ra, Rq, and Rz, as well as Shore-D hardness, were measured. Statistical analyses were performed using ANOVA and Duncan’s test. Results: Statistical analysis revealed that abrasive grit size significantly affected surface roughness (p < 0.001), with finer grits producing smoother surfaces. Wood species also had a significant effect on both roughness and hardness. Sanding had the greatest influence on Ra, Rq, and Rz parameters. Ebiara exhibited the smoothest surface, while Curupay showed the highest hardness (74.65). Conclusion: Surface roughness is primarily influenced by sanding grit, whereas hardness is determined by wood species. The results emphasize the importance of tailoring sanding procedures to the wood species in order to optimize surface quality and mechanical performance in industrial and decorative applications.
- MakaleYalnız künye2026Scopus SJRQ4CORRELATION BETWEEN THE CHEMICAL COMPOSITION OF WOOD AND THE INCREASING OF ITS CALORIFIC VALUE THROUGH HEAT TREATMENT; [CORRELAÇÃO ENTRE A COMPOSIÇÃO QUÍMICA DA MADEIRA E O AUMENTO DO PODER CALORÍFICO ATRAVÉS DO TRATAMENTO TÉRMICO]; [CORRELACIÓN ENTRE LA COMPOSICIÓN QUÍMICA DE LA MADERA Y EL AUMENTO DE SU PODER CALORÍFICO MEDIANTE TRATAMIENTO TÉRMICO]
Domingos, Idalina; Ferreira, Miguel; Ferreira, José; Dulyanska, Yuliya; Ayata, Umit; Esteves, Bruno
Introduction: The greatest importance of biomass lies in its Higher Heating Value (HHV), when considered for energy production. The calorific value is significantly affected by the changes in the chemical composition of the wood that occur during heat treatment. Objective: To understand the effect of heat treatment on the calorific value of the chemical constituents of two hardwoods: Sapelli and chestnut, and two softwoods: Scots pine and Siberian pine. Methods: The calorific value was determined by a Parr calorimeter – model 6400. The content of extractives was determined by successive Soxhlet extraction using about 3 g of each sample and 150 ml of dichloromethane, ethanol, and water as solvents. The extractives content was determined in accordance with TAPPI 204, and insoluble lignin by the Klason method Tappi T 222 om-02. For the determination of holocellulose, the acid chlorite method was used. Results: The calorific value of untreated wood ranged from 18.98 MJ/kg for chestnut to 20.35 MJ/kg for Siberian pine. Heat treatment resulted in an increase in the calorific value for most of the wood samples studied. Conclusion: The rise in HHV observed during heat treatment in softwoods and hardwoods is mainly due to the increase in lignin content, although dichloromethane extractives also play an important role.
- MakaleAçık Erişim2023Scopus SJRQ3Investigation of Use of Linden (Tilia tomentosa Moench.) Wood with UV System Varnish Application IN INDOOR Parquet Flooring
Ayata, Ümit; Esteves, Bruno; Domingos, Idalina; Ferreira, José; Tuncay Efe, Fatih; Türk, Mutlu; Çakicier, Nevzat; Gürleyen, Levent; Peker, Hüseyin
Linden wood is used in the making of musical instruments, agricultural hand tools, and in the furniture sector. In this study, the changes in glossiness (parallel (//) and perpendicular (⊥) to the fibers at 20°, 60°, and 85°, the pull-off adhesion test, color parameters (CIEL) and pendulum hardness (König method) of two different UV curable varnishes applied to linden (Tilia tomentosa Moench.) according to industrial application techniques and exposed to artificial weathering were investigated. According to the research results, while L*, ΔH*, and h° decreased with increasing weathering time in both varnish layers, ΔC*, b*, ΔE*, a*, and C* rose. The pendulum hardness grew for Method B but dwindled for Method A. A decrease was found in the adhesion tests for both varnish methods after artificial weathering. The glossiness was generally reduced due to artificial weathering for all the angles and for both directions, with the exception of 85º in Method A. The variance analysis and homogeneity groups showed that the changes in the adhesion, pendulum hardness, L*, a*, h°, C*, perpendicular and parallel to the fibers for 60° and 85° were found to be significantly different with artificial weathering for both methods.
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- MakaleAçık Erişim2023Scopus SJRQ2EFFECTS OF ARTIFICIAL WEATHERING ON THE SURFACE PROPERTIES OF COATED RADIATA PINE
Sahin, Sirri; Esteves, Bruno; Can, Ahmet; Sivrikaya, Hüseyin; Domingos, Idalina; Ferreira, José; Ayata, Ümit
Radiata pine boards were coated with two different methods A and B both beginning with a hydro primer and finishing with a mat oil but method A using an acrylic high gloss coating and method B three layers of an acrylic sealer in between. The samples were subjected to aging processes for 144 h, 288 h, and 432 h by using UV-A 340 nm lamps. The CIE L*a*b* and CIE L*C*H* coordinates were determined (L*, a*, b*, C*, ho*, ΔE*), gloss (perpendicular (⊥) and parallel (//) to the grain at 20°, 60°, and 85° angles) and surface adhesion strength via the pull-off method were tested before and after weathering. Results have shown that lightness (L*), decreases with weathering for both varnish applications with a higher decrease for the B coating system. Redness increased for both applications with no significant differences. At the same time there was a yellowing of the samples along the weathering period. Parallel and perpendicular gloss decreased for 20º and 60º angles while it increased for 85º angle. The adhesion strength of method A was higher and its decrease with weathering was smaller than for method B. Both varnish applications have proven to confer some protection against wood discoloration, but method A showed the best results and is therefore the best method to be used by radiata pine.
AtıfScopus2WoS2OpenAlex2İncele
- MakaleAçık Erişim2022Scopus SJRQ2EXTRACTIVES IN THERMALLY MODIFIED TROPICAL HARDWOODS
Esteves, Bruno; Ayata, Umit; Cruz-Lopes, Luísa; Brás, Isabel; Ferreira, José; Domingos, Idalina
Chemical composition of wood is known to change during thermal treatments. Two species grown in Turkey, afrormosia (Pericopsis elata) and duka (Tapirira guianensis) were heat treated according to Thermowood® method. Lignin, cellulose, hemicelluloses and extractives in dichloromethane, ethanol and water were determined. Wood extracts were analysed by gas chromatography with mass detection and existing compounds were identified by NIST17 database. Results show that hemicelluloses and cellulose content decreased for both heat-treated woods along the treatment while lignin percentage increased. The analysis of extractives has shown several compounds normally associated to lignin thermal degradation that increased along the treatment. At the same time several compounds associated to carbohydrate thermal degradation were found in all the extracts for both heat-treated woods. These founding have allowed the understanding of the degradation pattern of wood during thermal modification. There was not much difference between afrormosia and duka woods structural compounds behaviour along thermal modification. However, the variation of the amount of extractives along the treatment depended on the species.
AtıfScopus20WoS20OpenAlex16İncele
- MakaleAçık Erişim2021Scopus SJRQ3Effect of Heat Treatment on Shore-D Hardness of Some Wood Species
Esteves, Bruno; Sahin, Sırrı; Ayata, Ümit; Domingos, Idalina; Ferreira, José; Gürleyen, Levent
Hardness is an important wood property for several applications. Typically, it is necessary to use traditional methods, such as a universal test machine, to determine a wood’s hardness value. This work reports the hardness of some wood species before and after heat treatment (ThermoWood method) using the Shore-D hardness method. The Shore-D hardness value of untreated wood ranged between 35.3 for Limba wood and 77.2 for Santos wood. With heat treatment, hardness decreased, and the decrease was greater for samples that underwent harsher treatment (2 h at 212 °C). The decrease of hardness was highest for Sipo wood (14%) and the lowest for Afrormosia wood (2.5%). Analysis of variance tests showed that there was a significant difference between wood species, heat treatment, and the interaction between both variables at the chosen level of significance (P ≤ 0.05). Results showed that Shore-D hardness could be used to measure hardness directly in a production line or in small wood companies without using a universal test machine.
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- MakaleAçık Erişim2021Scopus SJRQ3Land Use Impact of Maritime Pine and Eucalypt: A Life Cycle Assessment Study
Ferreira, José; Esteves, Bruno; Ayata, Ümit; Cruz-Lopes, Luisa; Domingos, Idalina
The forestry sector in Portugal faces important challenges, resulting in an increased incidence of fires and the action of pathogens, which puts the sustainability of forest resources at risk. Due to the economic, social, and environmental importance of forests, this work assessed the land use environmental impact of maritime pine and eucalypt standing in Portuguese forests. SimaPro software was used to translate the inventory table results into land use impact category. The ILCD 2011 Midpoint+ method was chosen to assess the “land use” environmental impact that focuses on soil quality and its indicator (kg carbon deficit), which describes the changes in soil organic matter associated with land interventions. The results showed that for the first rotation time, the land use impact category per cubic meter of maritime pine is 18423 kg C deficit and 23430 kg C deficit for eucalypt, which means that the land use impact category of eucalypt is 27% higher than the impact of maritime pine.
AtıfScopus2WoS1OpenAlex1İncele
- MakaleAçık Erişim2020Scopus SJRQ2Calorific power improvement of wood by heat treatment and its relation to chemical composition
Domingos, Idalina; Ayata, Umit; Ferreira, José; Cruz-Lopes, Luisa; Sen, Ali; Sahin, Sirri; Esteves, Bruno
Chemical composition influences the calorific power of wood, mainly due to the calorific power of structural compounds and extractives. Heat treatment changes the chemical composition of treated wood. This work studies the relationship between chemical composition and calorific power improvement by heat treatment. Samples were heat-treated by the ThermoWood process ® for 1 h and 2 h. High heating value (HHV) and chemical composition; lignin, cellulose, hemicelluloses and extractives in dichloromethane, ethanol, and water were determined. The HHV of untreated wood ranged between 18.54-19.92 MJ/kg and increased with heat treatment for all the tested species. A positive linear correlation was found between HHV and Klason lignin (R2 = 0.60). A negative trend was observed for holocellulose, cellulose, and hemicelluloses content against HHV, but with low determination coefficients for linear regression. The best adjust for polysaccharides was found for hemicelluloses content. A positive correlation could be found for dichloromethane extractives (R2 = 0.04). The same was obtained in relation to ethanol extractives with R2 = 0.20. For water and total extractives, no clear positive or negative trends could be achieved. The results showed that the HHV of wood increased with heat treatment and that this increase was mainly due to the increase in lignin content.
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