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  • MakaleAçık Erişim2026Scopus SJRQ1
    Non-Destructive Intelligent Microwave Sensing of Water Content in Sand–Water Mixtures Using S-Parameter Features and PLS Regression

    Çakır, Mehmet

    The accurate and rapid estimation of water content in granular materials is important for geotechnical engineering, construction-material evaluation, agricultural monitoring, and non-destructive material assessment. This study presents a controlled laboratory feasibility framework for estimating water content in sand–water mixtures using microwave S-parameter measurements and physically interpretable features. Sixty measurements were acquired from six nominal mixture levels containing 0%, 5%, 10%, 15%, 20%, and 25% water by mass using a WR-229 waveguide-based fixture over 3.30–4.90 GHz. Descriptors were extracted from the raw and empty-reference-normalized S11 and S21 responses, including extrema, slopes, area-based indicators, band-averaged values, selected-frequency responses, and phase statistics. Ridge regression, partial least squares regression, support vector regression, Gaussian process regression, random forest, and gradient boosting regression were evaluated. The selected PLS model achieved RMSE = 3.56%, MAE = 2.92%, and R2 = 0.826 under leave-one-mixture-level-out group-wise cross-validation, which was used as the primary indicator of generalization to an unseen mixture level. The substantially lower error obtained under repeated-measurement leave-one-out cross-validation primarily reflects within-level repeatability under controlled conditions and should not be interpreted as evidence of universal calibration performance. The results demonstrate that magnitude- and phase-derived microwave descriptors, particularly transmission-based features, provide an interpretable and repeatable framework for water-content estimation under the specific sand type, sample geometry, water source, and laboratory conditions investigated. Further validation using independent preparation batches, different granular materials, measured water conductivity, temperature variation, and field-like conditions is required before practical deployment.

  • MakaleAçık Erişim2026Scopus SJRQ1
    A Single-Source Pilot Study of Machine Learning-Assisted Microwave S-Parameter Screening for Glucose Syrup and Water Adulteration in Grape Molasses

    Engin, Mustafa Alptekin; Cakir, Mehmet; Cakil, Turan

    Grape molasses, known as pekmez in Turkish, is a traditional concentrated fruit product that may be adulterated with cheaper sweeteners or water. This study evaluated broadband microwave S-parameter measurements as a rapid, non-destructive screening approach for detecting glucose syrup substitution and water dilution in grape molasses. Nine physical mixture groups were prepared, including pure grape molasses, glucose syrup–substituted mixtures at 5–30%, pure glucose syrup as an endpoint reference, and water-diluted mixtures at 10–30%. For each group, five consecutive technical measurements were recorded using a Libre vector network analyzer connected to a WR-229 waveguide-based two-port setup over 3.30–4.90 GHz. All mixtures were prepared from a single commercial grape molasses source and a single glucose syrup source; the results should therefore be interpreted as pilot-scale, single-source evidence rather than a generalizable screening method. Glucose syrup substitution produced a systematic upward shift in S11 resonance frequency. In the practical 0–30% range, S11 resonance frequency showed a strong linear relationship with glucose syrup content on the calibration data (R2 = 0.9955; inverse prediction error = 0.72 percentage points), though this reflects calibration fit rather than independently validated prediction accuracy. Water dilution produced stronger S21 attenuation. The detection principle is based on the complementary use of S11 resonance behavior for glucose syrup substitution and S21 transmission loss for water dilution. In group-blocked point-wise classification, the Ensemble Bagged Trees classifier achieved 88.79% accuracy and a macro-F1 score of 0.874. These results indicate that S11 and S21 provide complementary proof-of-concept indicators for controlled-mixture screening of grape molasses adulteration.

    • SDG 2 · Açlığa Son
  • MakaleAçık Erişim2025Scopus SJRQ1
    Validity and Reliability of a Novel AI-Based System in Athletic Performance Assessment: The Case of DeepSport †

    Aydemir, Burakhan; Aydoğan, Muhammed Talha; Boz, Emre; Kul, Murat; Kırkbir, Fatih; Özkara, Abdullah Bora

    This study aimed to examine the validity and reliability of the AI-based DeepSport application by comparing its outcomes with those from the reference device, OptoJump. The primary dependent variables measured were jump height and anaerobic power during vertical jump assessments. Twelve elite male basketball players voluntarily participated in the study (age = 21.53 ± 1.14 years; sports experience = 6.47 ± 1.01 years). DeepSport uses AI-based image processing from standard cameras, while OptoJump uses optical sensor technology. Both DeepSport and OptoJump systems were utilized to assess participants’ Countermovement Jump (CMJ) and Squat Jump (SJ) performances. A G*Power (version 3.1.9.7) analysis determined the required sample size, adopting a 95% confidence level, 90% test power, and an effect size of 0.25. Validity assessments were conducted using Bland-Altman plots and ordinary least products (OLP) regression analysis, while reliability was evaluated through intraclass correlation coefficient (ICC), coefficient of variation (CV), standard error of measurement (SEM), and smallest detectable change (SDC) analyses. DeepSport showed excellent reliability in CMJ and SJ tests with ICC values > 0.90, and CV ranged between 2.12% and 4.95%. Results were consistent with OptoJump, showing no significant differences according to t-test results (p > 0.05). Bland–Altman analyses indicated no systematic bias and random distribution. These findings confirm that both DeepSport and OptoJump devices demonstrate high reliability and consistency, suggesting their validity and reliability for use in athlete performance assessments by coaches and athletes.

    AtıfScopus4WoS3OpenAlex5
    ScopusWeb of SciencePubMedİncele
  • MakaleAçık Erişim2020Scopus SJRQ2
    High-throughput phenotyping approach for screening major carotenoids of tomato by handheld raman spectroscopy using chemometric methods

    Akpolat, Hacer; Barineau, Mark; Jackson, Keith A.; Akpolat, Mehmet Z.; Francis, David M.; Chen, Yu-Ju; Rodriguez-Saona, Luis E.

    Our objective was to develop a rapid technique for the non-invasive profiling and quantification of major tomato carotenoids using handheld Raman spectroscopy combined with pattern recognition techniques. A total of 106 samples with varying carotenoid profiles were provided by the Ohio State University Tomato Breeding and Genetics program and Lipman Family Farms (Naples, FL, USA). Non-destructive measurement from the surface of tomatoes was performed by a handheld Raman spectrometer equipped with a 1064 nm excitation laser, and data analysis was performed using soft independent modelling of class analogy (SIMCA)), artificial neural network (ANN), and partial least squares regression (PLSR) for classification and quantification purposes. High-performance liquid chromatography (HPLC) and UV/visible spectrophotometry were used for profiling and quantification of major carotenoids. Seven groups were identified based on their carotenoid profile, and supervised classification by SIMCA and ANN clustered samples with 93% and 100% accuracy based on a validation test data, respectively. All-trans-lycopene and β-carotene levels were measured with a UV-visible spectrophotometer, and prediction models were developed using PLSR and ANN. Regression models developed with Raman spectra provided excellent prediction performance by ANN (rpre = 0.9, SEP = 1.1 mg/100 g) and PLSR (rpre = 0.87, SEP = 2.4 mg/100 g) for non-invasive determination of all-trans-lycopene in fruits. Although the number of samples were limited for β-carotene quantification, PLSR modeling showed promising results (rcv = 0.99, SECV = 0.28 mg/100 g). Non-destructive evaluation of tomato carotenoids can be useful for tomato breeders as a simple and rapid tool for developing new varieties with novel profiles and for separating orange varieties with distinct carotenoids (high in β-carotene and high in cis-lycopene).

    • SDG 2 · Açlığa Son
    AtıfScopus40WoS32OpenAlex48
    ScopusWeb of SciencePubMedİncele
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AlanDeğerDil
creativeworkseries.issn1424-8220
dc.date.accessioned2026-10-29T19:08:07.980293713Z
dc.date.available2026-10-29T19:08:07.980293713Z
dc.identifier.urihttps://rdlopen.rawdatalibrary.net/r/bayburt/11184
dc.publisherMultidisciplinary Digital Publishing Institute (MDPI)
dc.rightsinfo:eu-repo/semantics/openAccess
dc.titleSensors