Sensitive and selective nitrite sensor based on CuCo2O4-rGO nanocomposite synthesized by one-pot electrochemical method in pastırma

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Özet

In this study, CuCo₂O₄-rGO nanostructures were synthesized by a one-pot electrochemical method on the surface of Pencil Graphite Electrode (PGE) for nitrite determination in pastırma, a traditional meat product. The developed modified electrode was used to determine the amount of nitrite in pastırma samples obtained from three different brands in the Turkish market. When the nitrite values obtained by the electrochemical method were compared with the spectrophotometric method, they showed 91.20 % to 100 % agreement. In addition, the physicochemical properties of pastırma samples, such as pH, moisture, protein, fat, and ash, were analysed, and it was determined that pH and moisture values are critical parameters for product quality. These results show that the developed electrode provides a practical and sensitive method for nitrite sensing.

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AlanDeğerDil
dc.contributor.authorAnlar Daldal, Pınar
dc.contributor.authorÖztürk Doğan, Hülya
dc.contributor.authorCinar Topcu, Kübra
dc.date.accessioned2026-10-29T19:07:52.859527542Z
dc.date.available2026-10-29T19:07:52.859527542Z
dc.date.issued2025
dc.description.abstractIn this study, CuCo₂O₄-rGO nanostructures were synthesized by a one-pot electrochemical method on the surface of Pencil Graphite Electrode (PGE) for nitrite determination in pastırma, a traditional meat product. The developed modified electrode was used to determine the amount of nitrite in pastırma samples obtained from three different brands in the Turkish market. When the nitrite values obtained by the electrochemical method were compared with the spectrophotometric method, they showed 91.20 % to 100 % agreement. In addition, the physicochemical properties of pastırma samples, such as pH, moisture, protein, fat, and ash, were analysed, and it was determined that pH and moisture values are critical parameters for product quality. These results show that the developed electrode provides a practical and sensitive method for nitrite sensing.
dc.identifier.articlenumber112550
dc.identifier.doi10.1016/j.diamond.2025.112550
dc.identifier.eissn1879-0062
dc.identifier.issn0925-9635
dc.identifier.scopus2-s2.0-105008214346
dc.identifier.urihttps://rdlopen.rawdatalibrary.net/r/bayburt/10932
dc.identifier.volume157
dc.identifier.wosWOS:001514004700001
dc.language.isoen
dc.publisherElsevier Ltd
dc.relation.ispartofDiamond and Related Materials
dc.rightsinfo:eu-repo/semantics/openAccess
dc.subjectCopper bismuthate
dc.subjectElectrochemical detection
dc.subjectNitrite sensor
dc.subjectPastırma
dc.subjectPencil graphite electrode
dc.subjectReduced graphene oxide
dc.subject.classificationMaterials Science, Multidisciplinary
dc.subject.classificationMaterials Science, Coatings & Films
dc.subject.classificationPhysics, Applied
dc.subject.classificationPhysics, Condensed Matter
dc.subject.classificationMaterials Science
dc.subject.classificationPhysics
dc.subject.otherBismuth compounds
dc.subject.otherChemical detection
dc.subject.otherCobalt compounds
dc.subject.otherCopper compounds
dc.subject.otherElectrochemical electrodes
dc.subject.otherGraphene
dc.subject.otherGraphite electrodes
dc.subject.otherMoisture
dc.subject.otherPhysicochemical properties
dc.subject.otherReduced Graphene Oxide
dc.subject.other%moisture
dc.subject.otherCopper bismuthate
dc.subject.otherELectrochemical detection
dc.subject.otherElectrochemical method
dc.subject.otherNitrite sensor
dc.subject.otherOne pot
dc.subject.otherPastırma
dc.subject.otherPencil graphite electrode
dc.subject.otherReduced graphene oxides
dc.subject.otherSynthesised
dc.subject.otherSpectrophotometry
dc.titleSensitive and selective nitrite sensor based on CuCo2O4-rGO nanocomposite synthesized by one-pot electrochemical method in pastırma
dc.typeArticle
rdl.citation.openalex2
rdl.citation.scopus2
rdl.citation.wos2
rdl.oa.statusclosed
rdl.oa.statusgreen
rdl.oa.urlhttps://hdl.handle.net/20.500.12403/5982
rdl.scopus.quartileQ1
rdl.source.indexSCOPUS
rdl.source.indexWOS
rdl.wos.indexScience Citation Index Expanded (SCI-EXPANDED)