Yazarlar

  • MakaleAçık Erişim2016Scopus SJRQ1
    Effects of grain size on room temperature deformation behavior of Zn–22Al alloy under uniaxial and biaxial loading conditions

    Cetin, M.E.; Demirtas, M.; Sofuoglu, H.; Cora, Ö.N.; Purcek, G.

    Effects of grain size on room temperature (RT) deformation behavior of superplastic Zn–22Al alloy under uniaxial and biaxial loading conditions were investigated. Two–step equal channel angular pressing (ECAP) and subsequent annealing processes were applied to the alloy in order to obtain microstructures with various grain sizes ranging from submicron to micron sizes. Grain size of 200 nm was achieved after ECAP of the alloy, and it was increased up to ~2.60 µm by annealing at 250 °C for different time periods. Changes in deformation behaviors of the alloy with various grain sizes were found to be in good agreement under the uniaxial tensile and biaxial Erichsen test conditions. Increasing grain size decreased both the maximum elongation under uniaxial deformation and limiting dome height (LDH) under biaxial deformation. The high elongation to failure and LDH values for the samples with submicron grain size were attributed to their high strain rate sensitivity.

    AtıfScopus20WoS19OpenAlex21
    ScopusWeb of Scienceİncele
  • MakaleAçık Erişim2016Scopus SJRQ1
    Effect of different processes on lamellar-free ultrafine grain formation, room temperature superplasticity and fracture mode of Zn-22Al alloy

    Demirtas, M.; Purcek, G.; Yanar, H.; Zhang, Z.J.; Zhang, Z.F.

    The Zn-22 wt.%Al was processed using five different selected routes including thermal, thermo-mechanical and severe plastic deformation (SPD) techniques in order to produce ultrafine grained (UFG) microstructure for achieving room temperature (RT) and high strain rate (HSR) superplasticity, and to compare the same set of the results. After all routes, the microstructural evolutions and RT uniaxial tensile tests at different strain rates ranging from 1 × 10-3 to 1 × 100 s-1 were investigated. The smallest grain size was achieved to be 300 nm after the thermo-mechanical process including conventional hot and cold rolling steps. However, the lamellar microstructure of the alloy was not completely eliminated during that process. On the other hand, equal-channel angular pressing (ECAP) as one of the SPD techniques decreased the grain size down to 400 nm with a lamellar-free microstructure. The maximum elongation value was achieved to be 330% with the sample tested at 1 × 10-3 s-1 after a thermo-mechanical process including conventional hot and cold rolling, and an aging stage between these rolling steps. It was found that lamellar-free microstructure causes higher superplastic elongation even if it has higher grain size compared to the sample having partially lamellar structure.

    AtıfScopus40WoS39
    ScopusWeb of Scienceİncele
  • MakaleYalnız künye2015Scopus SJRQ1
    Effect of equal-channel angular pressing on room temperature superplasticity of quasi-single phase Zn-0.3Al alloy

    Demirtas, M.; Purcek, G.; Yanar, H.; Zhang, Z.J.; Zhang, Z.F.

    Quasi-single phase (dilute) Zn-0.3Al alloy was subjected to severe plastic deformation via equal-channel angular extrusion/pressing (ECAE/P), and the effects of ECAP on its room temperature (RT) and high strain rate (HSR) superplasticity and deformation mechanism were investigated. Multi-pass ECAP may refine the coarse-grained microstructure into the fine grained (FG) one. The grain size of Zn-matrix phase decreased down to 2.0m after ECAP. Many spherical Al-rich precipitates decomposed and homogeneously distributed inside the matrix phase. They are ultrafine grained (UFG) α-particles with the grain sizes ranging from 50nm to ~200nm. This special microstructure having FG and UFG micro-constituents brought about an improvement in RT superplasticity even at HSRs. While multi-pass ECAP decreased flow stress of the alloy, its elongation to failure increased substantially depending on the initial strain rates. The maximum elongation was 1000% at a low strain rate of 10-4s-1, and 350% elongation was achieved at a high strain rate of 10-2s-1. Grain boundary sliding (GBS) was found to be the main deformation mechanism in region-II as the optimum superplastic region.

    AtıfScopus60WoS59OpenAlex55
    ScopusWeb of Scienceİncele