Sürdürülebilir Kalkınma Amaçları

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• MakaleYalnız künye2018Scopus SJRQ1/r/bayburt/12479
  High temperature superplasticity and deformation behavior of naturally aged Zn-Al alloys with different phase compositions

  Demirtas, M.; Kawasaki, M.; Yanar, H.; Purcek, G.

  Two Zn-Al alloys, eutectoid Zn-22Al and dilute Zn-0.3Al, were processed through equal-channel angular pressing (ECAP). The ECAP-processed alloys were subjected to long-term natural aging at room temperature for 120 days in order to investigate the effect of long-term natural aging on high-temperature superplasticity and the deformation behavior of these alloys. The grain size of the Zn-22Al alloy increased from 200 nm after ECAP to 400 nm after the natural aging process. The Zn-0.3Al alloy with a grain size of 1.3 µm after ECAP demonstrated a reasonably stable microstructure with the grain size of ~ 1.7 µm after long-term natural aging. The naturally aged ultrafine-grained (UFG) Zn-22Al alloy showed an excellent superplastic elongation of about 1800% at 200 °C. Grain boundary sliding was determined as the dominant deformation mechanism in this alloy. On the contrary, a considerably low elongation to failure of 230% was recorded in the naturally aged fine-grained (FG) Zn-0.3Al alloy at 150 °C, and dislocation creep was evaluated as the main deformation mechanism for this alloy. Detailed microstructural analyses showed that the FG Zn-0.3Al alloy was exposed to grain boundary corrosion during the natural aging process due to the presence of Al precipitates at grain boundaries whereas such formation was not observed in the UFG Zn-22% Al alloy. Grain boundary sliding was hindered by grain boundary corrosion and the cavity nucleation at the corroded grain boundaries caused a premature failure leading to such a low elongation in the Zn-0.3Al alloy.

  AtıfScopus30·WoS30·OpenAlex33

  İncele
• MakaleYalnız künye2016Scopus SJRQ1/r/bayburt/13857
  Optimization of strength, ductility and electrical conductivity of Cu-Cr-Zr alloy by combining multi-route ECAP and aging

  Purcek, G.; Yanar, H.; Demirtas, M.; Alemdag, Y.; Shangina, D.V.; Dobatkin, S.V.

  Properties of Cu-Cr-Zr alloy with ultrafine-grained (UFG) structure produced by equal-channel angular pressing (ECAP) via different routes have been investigated. Special attention was paid to the optimization of multi-functional structural, thermal, electrical and mechanical properties of the alloy by aging of UFG one. Multi-pass ECAP via different routes gives rise to the formation of a deformation-induced submicrocrystalline structure with the grain (subgrain) sizes in the range of 200-300. nm depending on applied routes which leads to high hardness and strength in the Cu-Cr-Zr alloy with reduced ductility. Amongst the applied routes, route-Bc was found to be the best processing path for achieving the lowest grain size, the highest hardness and strength. Aging of 8Bc-processed UFG samples increases the hardness and strength of Cu-Cr-Zr alloy while retaining an electrical conductivity comparable to that of aged coarse-grained (CG) one. A satisfactory electrical conductivity of 71%IACS without considerable loss of peak hardness was achieved after aging of 8Bc-processed UFG alloy at 425. °C for 240. min. The precipitation strengthened UFG alloy remains its stable behavior at elevated temperatures up to 450. °C.

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  AtıfScopus164·WoS147·OpenAlex151

  İncele
• MakaleAçık Erişim2016Scopus SJRQ1/r/bayburt/12536
  Effects of grain size on room temperature deformation behavior of Zn–22Al alloy under uniaxial and biaxial loading conditions

  Cetin, M.E.; Demirtas, M.; Sofuoglu, H.; Cora, Ö.N.; Purcek, G.

  Effects of grain size on room temperature (RT) deformation behavior of superplastic Zn–22Al alloy under uniaxial and biaxial loading conditions were investigated. Two–step equal channel angular pressing (ECAP) and subsequent annealing processes were applied to the alloy in order to obtain microstructures with various grain sizes ranging from submicron to micron sizes. Grain size of 200 nm was achieved after ECAP of the alloy, and it was increased up to ~2.60 µm by annealing at 250 °C for different time periods. Changes in deformation behaviors of the alloy with various grain sizes were found to be in good agreement under the uniaxial tensile and biaxial Erichsen test conditions. Increasing grain size decreased both the maximum elongation under uniaxial deformation and limiting dome height (LDH) under biaxial deformation. The high elongation to failure and LDH values for the samples with submicron grain size were attributed to their high strain rate sensitivity.

  AtıfScopus20·WoS19·OpenAlex21

  İncele
• MakaleAçık Erişim2015Scopus SJRQ1/r/bayburt/12532
  Improvement of high strain rate and room temperature superplasticity in Zn-22Al alloy by two-step equal-channel angular pressing

  Demirtas, M.; Purcek, G.; Yanar, H.; Zhang, Z.J.; Zhang, Z.F.

  The Zn-22Al alloy was subjected to equal-channel angular pressing (ECAP) to improve its high strain rate (HSR) superplasticity at room temperature (RT). A well-designed two-step ECAP process formed an ultrafine-grained (UFG) microstructure with an average grain size of 200nm as the lowest one obtained so far after ECAP processing of this alloy. Also, agglomerate- and texture-free microstructure with UFG Al-rich α- and Zn-rich η-grains separated mostly by high-angle grain boundaries (HAGBs) was produced by this process. The maximum RT elongation was achieved to be 400% with a strain rate sensitivity of 0.30 at a very high strain rate of 5×10-2s-1 after the two-step ECAP process. This elongation value is the highest one obtained at RT and at all strain rates for this alloy up to now. The current results demonstrate that such an improvement in superplasticity of Zn-22Al alloy after the two-step ECAP process can enhance its applications where RT and HSR superplasticity are strongly needed.

  AtıfScopus48·OpenAlex48

  İncele
• MakaleYalnız künye2015Scopus SJRQ1/r/bayburt/12454
  Effect of equal-channel angular pressing on room temperature superplasticity of quasi-single phase Zn-0.3Al alloy

  Demirtas, M.; Purcek, G.; Yanar, H.; Zhang, Z.J.; Zhang, Z.F.

  Quasi-single phase (dilute) Zn-0.3Al alloy was subjected to severe plastic deformation via equal-channel angular extrusion/pressing (ECAE/P), and the effects of ECAP on its room temperature (RT) and high strain rate (HSR) superplasticity and deformation mechanism were investigated. Multi-pass ECAP may refine the coarse-grained microstructure into the fine grained (FG) one. The grain size of Zn-matrix phase decreased down to 2.0m after ECAP. Many spherical Al-rich precipitates decomposed and homogeneously distributed inside the matrix phase. They are ultrafine grained (UFG) α-particles with the grain sizes ranging from 50nm to ~200nm. This special microstructure having FG and UFG micro-constituents brought about an improvement in RT superplasticity even at HSRs. While multi-pass ECAP decreased flow stress of the alloy, its elongation to failure increased substantially depending on the initial strain rates. The maximum elongation was 1000% at a low strain rate of 10-4s-1, and 350% elongation was achieved at a high strain rate of 10-2s-1. Grain boundary sliding (GBS) was found to be the main deformation mechanism in region-II as the optimum superplastic region.

  AtıfScopus60·WoS59·OpenAlex55

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