Sürdürülebilir Kalkınma Amaçları

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• MakaleYalnız künye2025Scopus SJRQ1/r/bayburt/11251
  Evaluation of the optical, structural, and morphological characteristics of a Sn-doped α-Fe2O3 thin film fabricated using RF and DC magnetron Co-sputtering technique

  Salari, Maryam Abdolahpour; Şenay, Volkan; Muğlu, Günay Merhan; Sarıtaş, Sevda; Kundakçı, Mutlu

  In this research, a Sn-doped hematite (α-Fe2O3) thin film on a glass substrate was synthesized using DC and RF magnetron sputtering techniques, and the physical features of the film were analyzed in detail. This study, conducted to investigate the effects of Sn doping on the hematite structure, evaluated the optical and morphological attributes of the thin film using advanced characterization techniques such as UV–VIS spectroscopy, Raman spectroscopy, XRD, SEM, EDS, and AFM. The optical band gap was determined from absorption measurement and calculated to be 2.12 eV. Raman spectroscopy results revealed various characteristic peaks between 100 cm−1 and 1500 cm−1. A strong (214) diffraction peak confirms the enhanced hematite phase formation in the thin film. The crystallite size of the Sn-doped thin film, calculated via Scherrer's formula, is 20 nm. SEM images showed that the thin film exhibited a smooth and homogeneous surface morphology on the glass substrate. According to the EDS results, the atomic doping ratio of Sn in Fe2O3 is 2.84 %. Additionally, AFM analysis confirmed that the Sn-doped α-Fe2O3 thin film had a smooth surface, as indicated by a low RMS (Root Mean Square) roughness value of 8.11 nm. These properties suggest that the thin film could be suitable for optoelectronic applications. The study emphasizes the potential of Sn-doped α-Fe2O3 thin films, particularly for optoelectronic and photocatalytic devices, and underscores the need for further investigation of these materials. Furthermore, it was concluded that these materials should be considered in a broader context for their potential use in various technological applications.

  AtıfScopus23·WoS22·OpenAlex25

  İncele
• MakaleAçık Erişim2024Scopus SJRQ1/r/bayburt/11697
  Analysis of optical, structural, and morphological properties of a Ti-doped α-Fe2O3 thin film produced through RF and DC magnetron Co-sputtering

  Abdolahpour Salari, Maryam; Merhan Muğlu, Günay; Şenay, Volkan; Sarıtaş, Sevda; Kundakçı, Mutlu

  In this study, a Titanium (Ti) doped α-Fe2O3 (hematite) thin layer was synthesized onto a glass substrate, employing the simultaneous DC and RF magnetron sputtering method. The investigation focused on examining specific physical properties of the film. The optical, structural, morphological, and elemental features of the resulting Ti-doped α-Fe2O3 thin film were characterized using different characterization techniques. The XRD studies indicated a rhombohedral crystal structure in the studied thin film. The calculation of the Eg value for the thin film, based on absorption measurements, resulted in a value of 2.19 eV. Raman peaks were identified within the range of 218 cm−1 to 1300 cm−1. According to SEM images, the thin film exhibited a uniform surface morphology across the substrate. AFM images revealed a low root mean square (RMS) roughness value, indicating a smooth Ti:Fe2O3 thin film surface.

  AtıfScopus24·WoS25·OpenAlex29

  İncele
• MakaleYalnız künye2021Scopus SJRQ1/r/bayburt/12135
  The effects of fuel type onto the structural, morphological, magnetic and photocatalytic properties of nanoparticles in the synthesis of cobalt ferrite nanoparticles with microwave assisted combustion method

  Karakas, İbrahim Hakkı

  In this experimental study, the synthesis of cobalt ferrite nanoparticles, one of the most important types of ferromagnetic spinel ferrite materials was realized by using a method known as microwave assisted combustion method. The effects of the substance used as fuel on the structural, morphological, magnetic and photocatalytic properties of synthesized nanoparticles were investigated. Firstly, samples were prepared using urea, glycine and citric acid as fuel and then the samples were comprehensively characterized by advanced analysis techniques such as XRD, FT-IR, TEM, SEM, VSM, BET. Moreover, the usability of the obtained nanoparticles in photocatalytic degradation process of Procion Yellow H-E3G textile dye as photocatalyst was investigated. The results obtained indicate that the fuel used is highly effective on various properties of the synthesized materials. From the experiments performed to evaluate the photocatalytic performances of the nanoparticles, it was observed that each of the three different fuel matters used for the synthesis of nanoparticles were highly effective on the photocatalytic degradation of the organic pollutant. Furthermore, almost all the dye content in solution was completely removed at the end of the experimental period which lasted for 90 min.

  AtıfScopus50·WoS44·OpenAlex51

  İncele
• MakaleYalnız künye2020Scopus SJRQ1/r/bayburt/12116
  Thin films derived from Zn(Al)O mixed metal oxides nanoparticles dispersed in polyethylene glycol: Structural, morphological and optical properties

  El Hassani, Kaoutar; Bayram, Ozkan; Anouar, Abdellah; Mavi, Ahmet

  In this study, Zn(Al)O thin films were produced using colloidal solution of Zn(Al)O nanoparticles dispersed in polyethylene glycol (PEG). Zn(Al)O mixed metal oxides were obtained by a simple pyrolysis of Zn–Al containing layered double hydroxide materials with different Al content. Survey of textural analysis of Zn(Al)O mixed oxides displayed characteristic peaks of ZnO structure. The calculated ratios of lattice parameters c/a were found to be 1.61 and 1.60 for 3-ZAO and 5-ZAO, respectively. The optical transmittance of the prepared thin films was not significantly affected by the increase in Al content; however, this increase changed the optical band gap from 3.27 eV to 3.33 eV. ZAO thin films, which are both cost-effective with good optical properties, have the potential to be an alternative to those used in many optical devices lately.

  AtıfScopus4·WoS3·OpenAlex4

  İncele
• MakaleYalnız künye2019Scopus SJRQ1/r/bayburt/13763
  Vertically oriented graphene nano-sheets grown by plasma enhanced chemical vapor deposition technique at low temperature

  Bayram, Ozkan; Simsek, Onder

  In this study, it was aimed to obtain vertically-oriented graphene nano-sheets (VGNs) on copper foils using CH 4 gas as the precursor material by means of plasma enhanced chemical vapor deposition (PECVD) technique. VGNs were obtained at 50 W, 75 W and 100 W Radio Frequency (RF) powers by this technique and the effect of RF power on the morphological structure of graphene layers was investigated. VGNs were also analyzed by Raman spectroscopy, scanning electron microscopy (SEM) and water contact angle (WCA) measurements. The SEM images showed that the VGNs became more tightly packed with the increase of RF power and thus these coating parameters had a significant effect on the morphological structure. WCA analyzes for VGNs were also performed and it was found that VGNs obtained at 100 W RF power had higher contact angle value than the other RF powers. These VGNs, which have both large surface area and optically transparent, are thought to be materials that have the potential to be used in supercapacitors and solar cells.

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  AtıfScopus19·WoS17·OpenAlex19

  İncele
• MakaleYalnız künye2019Scopus SJRQ1/r/bayburt/11938
  A study on 3D graphene synthesized directly on Glass/FTO substrates: Its Raman mapping and optical properties

  Bayram, Ozkan

  In this study, vertically oriented (3D) graphene nanostructures (VGN) were obtained on Glass and Fluorine doped tin oxide (FTO) substrates at relatively low temperatures (approaximatelly at 400 °C) by using plasma enhanced chemical vapor deposition (PECVD) technique. VGNs were characterized using Raman, Uv–Vis and SEM spectroscopies, respectively. Raman spectroscopy showed that growth temperature significantly affected VGN formation and film quality. The layer structures of these VGNs were also confirmed by Raman mapping. The most important data obtained from this study is that although the applied radio frequency (RF) power is the same, the growth temperature significantly affects the graphene formation and morphologies. This was attributed to the fact that CH4 decomposition was very difficult at low temperatures. The optical transmittance of VGNs ranged from 50% to 95% (at 550 nm wavelength) and their electrical conductivity was also determined to be between 5.94 kohm/sqr and 11.2 kohm/sqr. The electrical and optical properties of VGNs, which have a large surface area, indicated that they may be an alternative material for sensor, solar cell and supercapacitor applications.

  AtıfScopus19·WoS18·OpenAlex20

  İncele
• MakaleYalnız künye2018Scopus SJRQ1/r/bayburt/12466
  Conjugated polythiophene/Ni doped ZnO hetero bilayer nanocomposite thin films: Its structural, optical and photoluminescence properties

  Bayram, Ozkan

  In this study, synthesis and characterization of plasma polymerized Thiophene/ Nickel doped Zinc Oxide (PTNZO) bilayer nanocomposite films were carried out. Nickel doped zinc oxide (NZO) thin films were obtained by magnetron sputtering technique on glass substrates at 40 W Radio Frequency (RF) power. Plasma polymerized Thiophene (PT) thin films were deposited on the NZO thin films obtained on the glass substrate by Radio Frequency (RF) plasma polymerisation technique. X-Ray Diffraction (XRD), Scanning Electron Microscopy (SEM), FTIR and Photoluminescence (PL) analyzes were performed for the characterization of PTNZO hetero bilayer nanocomposite films. In the XRD spectra of PTNZO bilayer nanocomposite thin films, (002) planes were determined as the most basic peak, and it was determined that the intensity of this peak, changed depending on the RF power of polymer thin films. Optical properties of nanocomposite thin films such as transmittance, absorbance and optical band gap were determined by UV–Vis spectroscopy. Optical band gap for PTNZO nanocomposites were 2.72 eV, 2.34 eV, and 2.45 eV, respectively, with increasing RF power. For NZO thin films, this value is 3.12 eV. The optical band gaps calculated from the absorption and transmittance spectra obtained using UV–visible spectroscopy had a good compatibility with those of the optical band spectra calculated from the PL spectra. The tetragonal wurtzite structure of the NZO thin films was examined by SEM analysis. The grain size of NZO nanostructure was found to be approximately 59 nm.

  AtıfScopus9·WoS9·OpenAlex9

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